Main Sensor
The sensor is the heart of the Lumen spectrometer. It converts the optical signal from the interferometer into an electrical signal usable by the acquisition chain.
Operating Principle
Section titled “Operating Principle”The sensor used in Lumen is a deuterated triglycine sulfate (DTGS) pyroelectric detector. It measures the infrared beam intensity after it passes through the sample and the Michelson interferometer.
IR Source → Interferometer → Sample → DTGS Sensor → ADC → ProcessingDetection Chain
Section titled “Detection Chain”- Optical window: potassium bromide (KBr), transparency from 2.5 to 25 µm.
- Sensitive element: DTGS crystal, 2 mm diameter.
- Preamplifier: low-noise transimpedance amplifier, gain of 10⁶ V/A.
- Low-pass filter: 5 kHz cutoff for high-frequency noise rejection.
Technical Specifications
Section titled “Technical Specifications”| Parameter | Value |
|---|---|
| Spectral range | 2.5 – 25 µm |
| Sensitivity (D*) | 1.5 × 10⁸ cm·Hz½/W |
| Active area | 2 mm |
| Max output voltage | ±5 V |
| Noise Equivalent (NEP) | 0.5 nW/Hz½ |
| Response time | < 10 ms |
| Temperature range | 10 – 40 °C |
Calibration
Section titled “Calibration”Wavelength Calibration
Section titled “Wavelength Calibration”Use a polystyrene reference film:
- Place the film in the sample holder.
- Acquire a spectrum with 32 scans.
- Check the characteristic peaks at 1601 cm⁻¹, 1493 cm⁻¹, and 1028 cm⁻¹.
- Adjust the correction factor if the deviation exceeds ±2 cm⁻¹.
Intensity Calibration
Section titled “Intensity Calibration”Intensity calibration is performed with a reference mirror (reflectivity > 98% in the mid-IR range):
def calibrate_intensity(raw_spectrum, reference_spectrum): """Calibrate the raw spectrum against the reference spectrum.""" import numpy as np return raw_spectrum / reference_spectrum * 100 # % transmissionMaintenance
Section titled “Maintenance”- Window cleaning: optical cloth + isopropanol, once a month.
- Baseline check: empty acquisition (no sample) every 50 measurements.
- Desiccant replacement: every 3 months to prevent moisture absorption by the KBr.
Electronic Interfacing
Section titled “Electronic Interfacing”The sensor communicates with the acquisition board via a 50 Ω BNC connector. The signal is digitized by a 16-bit ADC at 100 kS/s (AD7680).
DTGS Sensor ──┬── V_out (BNC) ──→ ADC AD7680 ──→ Microcontroller └── GNDLorem ipsum dolor sit amet, consectetur adipiscing elit. Sed do eiusmod tempor incididunt ut labore et dolore magna aliqua. Ut enim ad minim veniam, quis nostrud exercitation ullamco laboris nisi ut aliquip ex ea commodo consequat. Duis aute irure dolor in reprehenderit in voluptate velit esse cillum dolore eu fugiat nulla pariatur. Excepteur sint occaecat cupidatat non proident, sunt in culpa qui officia deserunt mollit anim id est laborum.
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